6U6U

IL36R extracellular domain in complex with BI655130 Fab

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06DA
Synchrotron site	SLS
Beamline	X06DA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2014-05-16
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	1.000000
Spacegroup name	P 21 21 21
Unit cell lengths	60.698, 70.663, 233.268
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	36.990 - 2.310
R-factor	0.1802
Rwork	0.179
R-free	0.20210
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1g0y
RMSD bond length	0.009
RMSD bond angle	1.087
Data reduction software	XDS
Data scaling software	d*TREK
Phasing software	PHASER
Refinement software	PHENIX (1.9_1692)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	116.630	2.318
High resolution limit [Å]	2.310	2.310
Rmerge	0.090	0.921
Number of reflections	45094	45094
<I/σ(I)>	12.7	2
Completeness [%]	100.0	100
Redundancy	6.7	6.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	1.6 M Na3C6H5O7