6TIZ
DROSOPHILA GDP-TUBULIN Y222F MUTANT
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 2 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-06-13 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.98 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 66.176, 126.732, 250.364 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 32.000 - 2.197 |
R-factor | 0.1766 |
Rwork | 0.175 |
R-free | 0.20850 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 3ryc |
RMSD bond length | 0.008 |
RMSD bond angle | 0.960 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | BUSTER |
Refinement software | BUSTER (2.10.3 (3-OCT-2019)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 63.370 | 2.230 |
High resolution limit [Å] | 2.197 | 2.197 |
Number of reflections | 107685 | 29817 |
<I/σ(I)> | 12.8 | 1.6 |
Completeness [%] | 99.5 | |
Redundancy | 9.4 | |
CC(1/2) | 0.998 | 0.651 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293 | PEG1500, LISO4, PIPES BUFFER, PH 6.8 |