6SEV

Structure of Dps from Listeria innocua soaked with 10 mM zinc for 120 minutes

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALBA BEAMLINE XALOC
Synchrotron site	ALBA
Beamline	XALOC
Temperature [K]	100
Detector technology	PIXEL
Collection date	2015-01-01
Detector	DECTRIS PILATUS3 S 6M
Wavelength(s)	1
Spacegroup name	P 41 21 2
Unit cell lengths	84.831, 84.831, 267.358
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	2.020 - 2.000
Structure solution method	MOLECULAR REPLACEMENT
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	MOLREP
Refinement software	PHENIX

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.100
High resolution limit [Å]	2.000	2.000
Rmerge		2.300
Number of reflections	66812	10607
<I/σ(I)>	15.6
Completeness [%]	99.7
Redundancy	16.2
CC(1/2)	0.990	0.330

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		294	30% PEG1500, 100 mM Hepes pH 7.5