6PV4
Structure of CpGH84A
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-12-14 |
Detector | RAYONIX MX-300 |
Wavelength(s) | 0.97965 |
Spacegroup name | P 1 |
Unit cell lengths | 92.090, 92.110, 103.080 |
Unit cell angles | 95.74, 110.52, 119.71 |
Refinement procedure
Resolution | 75.450 - 2.200 |
R-factor | 0.2042 |
Rwork | 0.202 |
R-free | 0.24810 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2v5c |
RMSD bond length | 0.005 |
RMSD bond angle | 1.198 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0253) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 78.000 | 2.320 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.167 | 0.386 |
Rpim | 0.113 | 0.262 |
Number of reflections | 129154 | 18702 |
<I/σ(I)> | 7.7 | 5.6 |
Completeness [%] | 98.1 | 97.3 |
Redundancy | 2.7 | 2.7 |
CC(1/2) | 0.929 | 0.454 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | 14% PEG3350, 0.15 M CaCl2 and 20 mM octyl-beta-D-glucopyranoside |