6OHH
Structure of EF1p2_mFAP2b bound to DFHBI
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2018-08-13 |
Detector | RIGAKU SATURN 944+ |
Wavelength(s) | 1.54 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 36.350, 35.564, 86.596 |
Unit cell angles | 90.00, 90.68, 90.00 |
Refinement procedure
Resolution | 25.420 - 2.100 |
R-factor | 0.1725 |
Rwork | 0.169 |
R-free | 0.20090 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.004 |
RMSD bond angle | 0.859 |
Data scaling software | HKL-2000 |
Phasing software | PHASER (2.7.16) |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 30.000 | 30.000 | 2.140 |
High resolution limit [Å] | 2.100 | 5.690 | 2.100 |
Rmerge | 0.025 | 0.020 | 0.055 |
Rmeas | 0.030 | 0.023 | 0.068 |
Rpim | 0.016 | 0.012 | 0.040 |
Number of reflections | 13078 | 706 | 570 |
<I/σ(I)> | 16.6 | ||
Completeness [%] | 98.9 | 99.4 | 86.2 |
Redundancy | 3.6 | 3.5 | 2.8 |
CC(1/2) | 1.000 | 0.996 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 298 | 0.1 M HEPES pH 7.5, 25% PEG3350 |