6O4P

The crystal structure of the interleukin 11 alpha receptor

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	AUSTRALIAN SYNCHROTRON BEAMLINE MX2
Synchrotron site	Australian Synchrotron
Beamline	MX2
Temperature [K]	100
Detector technology	CCD
Collection date	2017-02-27
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.9537
Spacegroup name	P 65 2 2
Unit cell lengths	171.456, 171.456, 107.944
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	45.674 - 3.429
R-factor	0.2464
Rwork	0.244
R-free	0.29840
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.002
RMSD bond angle	0.581
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHASER
Refinement software	PHENIX ((1.13_2998: ???))

Data quality characteristics

	Outer shell
Low resolution limit [Å]	3.700
High resolution limit [Å]	3.430
Completeness [%]	98.5
CC(1/2)	0.436

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	8	293	1.6 M Ammonium sulfate, 0.02 M NaCl, 67 mM NDSB-195, 0.1 M HEPES pH 8.0