6NWS
RORgamma Ligand Binding Domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.2 |
Synchrotron site | ALS |
Beamline | 5.0.2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-12-14 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 1.000 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 60.805, 60.805, 160.650 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 56.868 - 2.440 |
R-factor | 0.2528 |
Rwork | 0.250 |
R-free | 0.29740 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5vb3 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.535 |
Data reduction software | XDS |
Data scaling software | xia2 |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 56.870 | 56.870 |
High resolution limit [Å] | 2.440 | 2.440 |
Number of reflections | 11958 | |
<I/σ(I)> | 9.21 | |
Completeness [%] | 99.1 | |
Redundancy | 16 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.4 | 295 | 0.1 M sodium phosphate, pH 7.4, 0.5-0.7 M sodium chloride, 4-6% PEG4000, 3% DMSO |