6MWL

LasR LBD:mBTL complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU RUH3R
Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	2013-05-15
Detector	RIGAKU RAXIS IV++
Wavelength(s)	1.0
Spacegroup name	P 1 21 1
Unit cell lengths	52.073, 67.325, 53.785
Unit cell angles	90.00, 117.07, 90.00

Refinement procedure

Resolution	20.200 - 1.500
R-factor	0.1924
Rwork	0.191
R-free	0.22150
RMSD bond length	0.007
RMSD bond angle	1.140
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHENIX
Refinement software	PHENIX (1.8.1_1168)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	20.200	1.550
High resolution limit [Å]	1.500	1.500
Number of reflections	52957
<I/σ(I)>	18.5
Completeness [%]	99.1
Redundancy	3.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	200 mM magnesium nitrate, 20% PEG3350