6MVX
NavAb Voltage-gated Sodium Channel, I217C, in Complex with Class 1C Anti-arrhythmic Flecainide
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.1 |
Synchrotron site | ALS |
Beamline | 8.2.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-12-18 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.0 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 177.525, 177.687, 192.923 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.855 - 3.455 |
R-factor | 0.236 |
Rwork | 0.230 |
R-free | 0.26290 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3rvy tetramer |
RMSD bond length | 0.004 |
RMSD bond angle | 0.670 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.579 |
High resolution limit [Å] | 3.455 | 3.455 |
Rmerge | 0.157 | |
Number of reflections | 39868 | |
<I/σ(I)> | 8.75 | |
Completeness [%] | 99.9 | |
Redundancy | 6.3 | |
CC(1/2) | 0.431 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | 1.8 M Ammonium Sulfate 100 mM Sodium Acetate, pH 5.0 100 uM Flecainide |