6LHD
Crystal structure of p53/BCL-xL fusion complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2018-11-17 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 72.221, 68.850, 75.028 |
Unit cell angles | 90.00, 110.27, 90.00 |
Refinement procedure
Resolution | 49.217 - 2.499 |
R-factor | 0.2048 |
Rwork | 0.202 |
R-free | 0.26010 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3kmd 2yxj |
RMSD bond length | 0.004 |
RMSD bond angle | 0.592 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.11.1_2575) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.599 |
High resolution limit [Å] | 2.499 | 2.499 |
Rmerge | 0.116 | 0.633 |
Rmeas | 0.139 | 0.755 |
Number of reflections | 23478 | 2185 |
<I/σ(I)> | 7.89 | 2.46 |
Completeness [%] | 97.0 | |
Redundancy | 3.4 | |
CC(1/2) | 0.899 | 0.766 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 291.15 | 0.2M sodium malonate pH 7.0, 20%(w/v) polyethylene glycol 3,350 |