6K73
Chaperone-tip adhesin complex is vital for synergistic activation of CFA/I fimbriae biogenesis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-04-20 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97776 |
Spacegroup name | H 3 2 |
Unit cell lengths | 217.158, 217.158, 177.091 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 29.517 - 2.774 |
R-factor | 0.2265 |
Rwork | 0.225 |
R-free | 0.25970 |
Structure solution method | MOLECULAR REPLACEMENT |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.870 |
High resolution limit [Å] | 2.774 | 2.774 |
Rmerge | 0.111 | 0.562 |
Number of reflections | 40388 | 10 |
<I/σ(I)> | 12.29 | |
Completeness [%] | 99.7 | 99.5 |
Redundancy | 7.5 | 5.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 2%PEG8000, 0.1M imidazole malate, 1.04M Li2SO4, 0.01M GSSG-GSH |