6I5Q
Papaver somniferum O-methyltransferase 1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-09-19 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9795 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 112.004, 112.004, 304.820 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 97.000 - 3.050 |
R-factor | 0.21247 |
Rwork | 0.210 |
R-free | 0.25569 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1kyz |
RMSD bond length | 0.007 |
RMSD bond angle | 1.597 |
Data reduction software | xia2 |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 97.000 | 3.170 |
High resolution limit [Å] | 3.050 | 3.050 |
Rmerge | 0.151 | 1.607 |
Rpim | 0.052 | 0.561 |
Number of reflections | 43285 | 4464 |
<I/σ(I)> | 10.7 | |
Completeness [%] | 100.0 | 100 |
Redundancy | 9.9 | 10 |
CC(1/2) | 0.997 | 0.592 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 291 | PEG 3350, sodium citrate, bis-tris propane |