6I2Y
Human STK10 bound to Foretinib
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-09-12 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9282 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 50.930, 95.330, 132.860 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 54.502 - 2.560 |
R-factor | 0.2639 |
Rwork | 0.263 |
R-free | 0.28280 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.003 |
RMSD bond angle | 0.674 |
Data reduction software | XDS |
Data scaling software | Aimless (0.5.27) |
Phasing software | REFMAC |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 54.500 | 54.500 | 2.630 |
High resolution limit [Å] | 2.560 | 11.450 | 2.560 |
Rmerge | 0.089 | 0.031 | 1.501 |
Rmeas | 0.098 | 0.035 | 1.652 |
Rpim | 0.039 | 0.014 | 0.683 |
Total number of observations | 135087 | 1495 | 8850 |
Number of reflections | 21454 | 297 | 1534 |
<I/σ(I)> | 11.2 | 34.8 | 1.1 |
Completeness [%] | 99.4 | 98 | 99.4 |
Redundancy | 6.3 | 5 | 5.8 |
CC(1/2) | 0.999 | 0.998 | 0.668 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | 0.2M sodium chloride -- 25% PEG3350 -- 0.1M bis-tris pH 5.5 |