6HP8
Crystal structure of DPP8 in complex with Val-BoroPro
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-12-11 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.99992 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 163.163, 245.317, 261.588 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.620 - 2.500 |
R-factor | 0.20463 |
Rwork | 0.203 |
R-free | 0.22785 |
RMSD bond length | 0.002 |
RMSD bond angle | 0.916 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (7.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.620 | 2.560 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmeas | 0.145 | 1.560 |
Number of reflections | 179844 | |
<I/σ(I)> | 15.64 | |
Completeness [%] | 99.9 | 99.6 |
Redundancy | 8.4 | 8.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 6.75 | 293 | 0.46 M Na-citrate |