6HN6
A revisited version of the apo structure of the ligand-binding domain of the human nuclear receptor RXR-ALPHA
Replaces: 1LBDExperimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | LURE BEAMLINE DW32 |
| Synchrotron site | LURE |
| Beamline | DW32 |
| Temperature [K] | 290 |
| Detector technology | IMAGE PLATE |
| Collection date | 1994-03-09 |
| Detector | MARRESEARCH |
| Wavelength(s) | 0.98 |
| Spacegroup name | P 63 2 2 |
| Unit cell lengths | 110.800, 110.800, 109.900 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 7.990 - 2.710 |
| R-factor | 0.176 |
| Rwork | 0.173 |
| R-free | 0.23100 |
| Structure solution method | MIR |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.090 |
| Data reduction software | XDS (MARXDS) |
| Data scaling software | XSCALE (MARSCALE) |
| Phasing software | MLPHARE |
| Refinement software | BUSTER (2.10.2) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 7.990 | 3.030 |
| High resolution limit [Å] | 2.710 | 2.710 |
| Number of reflections | 9164 | 2597 |
| <I/σ(I)> | 4.9 | |
| Completeness [%] | 84.7 | 83.03 |
| Redundancy | 4.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7 | 289 | 0.45 M AMMONIUM CITRATE, 30 mM KCl, 4% GLYCEROL, 5 mM CHAPS, pH 7.0 |
