6HHQ
Crystal structure of compound C45 bound to the yeast 80S ribosome
This is a non-PDB format compatible entry.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SOLEIL BEAMLINE PROXIMA 1 |
| Synchrotron site | SOLEIL |
| Beamline | PROXIMA 1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-06-20 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 1.0 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 303.770, 287.950, 435.450 |
| Unit cell angles | 90.00, 98.96, 90.00 |
Refinement procedure
| Resolution | 54.708 - 3.100 |
| R-factor | 0.217667239898 |
| Rwork | 0.217 |
| R-free | 0.26447 |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.354 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHENIX |
| Refinement software | PHENIX (dev_2450) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 55.000 | 3.200 |
| High resolution limit [Å] | 3.100 | 3.100 |
| Rmeas | 0.422 | |
| Number of reflections | 1332963 | |
| <I/σ(I)> | 7.65 | 1.2 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 16.4 | |
| CC(1/2) | 0.992 | 0.504 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7 | 277 | PEG 20K, KSCN, Mg Acetate, Tris-Acetate, Glycerol, Spermidine |
