6HB4
TFAM in Complex with Site-Y
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-2 |
Synchrotron site | ESRF |
Beamline | ID23-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-09-10 |
Detector | DECTRIS PILATUS3 X 2M |
Wavelength(s) | 0.93928 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 157.669, 140.622, 108.919 |
Unit cell angles | 90.00, 130.73, 90.00 |
Refinement procedure
Resolution | 43.050 - 3.050 |
R-factor | 0.1924 |
Rwork | 0.190 |
R-free | 0.23580 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3tq6 |
RMSD bond length | 0.012 |
RMSD bond angle | 1.520 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | BUSTER (2.11.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.700 | 3.140 |
High resolution limit [Å] | 3.050 | 3.050 |
Number of reflections | 34352 | 2796 |
<I/σ(I)> | 19.4 | |
Completeness [%] | 100.0 | |
Redundancy | 13.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293 | 23-28% PEG 3350, 0.08-0.2M ammonium acetate, and 0.1 M bis-Tris pH 6.5 or Hepes pH 7.5 |