6GEI
TEAD4 (216-434);E263A+Y429F COMPLEXED WITH YAP PEPTIDE (60- 100);S94A AND MYRISTOATE (COVALENTLY BOUND TO LYS344, NOT CYS367!) AT 1.65A (P41212 CRYSTAL FORM); MYRISTOYLATION WAS DONE BY ADDING MYR-COA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-02-03 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.99994 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 59.036, 59.036, 158.969 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.720 - 1.650 |
R-factor | 0.2301 |
Rwork | 0.229 |
R-free | 0.24830 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6ge3 |
RMSD bond length | 0.006 |
RMSD bond angle | 0.960 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.720 | 1.690 |
High resolution limit [Å] | 1.650 | 1.650 |
Rmerge | 0.079 | 0.910 |
Rmeas | 0.083 | 0.947 |
Total number of observations | 447910 | |
Number of reflections | 34774 | |
<I/σ(I)> | 24.7 | 3.2 |
Completeness [%] | 99.9 | 100 |
Redundancy | 12.9 | 13.4 |
CC(1/2) | 1.000 | 0.882 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 298 | 20% PEG 3350, 0.2M Na acetate |