6FYT
Structure of H1 (A/solomon Islands/3/06) Influenza Hemagglutinin in complex with SD38
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 23-ID-D |
| Synchrotron site | APS |
| Beamline | 23-ID-D |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2013-10-20 |
| Detector | MARRESEARCH |
| Wavelength(s) | 1.03316 |
| Spacegroup name | P 63 |
| Unit cell lengths | 107.540, 107.540, 198.330 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 47.268 - 2.800 |
| R-factor | 0.2021 |
| Rwork | 0.200 |
| R-free | 0.23460 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.003 |
| RMSD bond angle | 0.593 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | PHENIX ((dev_2614: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.900 |
| High resolution limit [Å] | 2.800 | 2.800 |
| Rpim | 0.060 | 0.530 |
| Number of reflections | 31685 | 3141 |
| <I/σ(I)> | 10.3 | 2 |
| Completeness [%] | 99.0 | 98 |
| Redundancy | 3.5 | 3.5 |
| CC(1/2) | 1.000 | 0.690 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 8 | 277 | 0.2 M calcium acetate, 10 % PEG800 and o.1 M imidazole pH 8.0 |
