6FS2
MCL1 in complex with indole acid ligand
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-02-09 |
Detector | RIGAKU SATURN 944 |
Wavelength(s) | 1.54 |
Spacegroup name | P 1 |
Unit cell lengths | 46.710, 46.710, 47.493 |
Unit cell angles | 74.74, 74.74, 61.83 |
Refinement procedure
Resolution | 45.200 - 2.550 |
R-factor | 0.192 |
Rwork | 0.186 |
R-free | 0.25400 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.050 |
Data reduction software | iMOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | BUSTER (2.11.6) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.220 | 2.750 |
High resolution limit [Å] | 2.550 | 2.550 |
Number of reflections | 10721 | |
<I/σ(I)> | 8.55 | 2.05 |
Completeness [%] | 97.2 | 96.1 |
Redundancy | 2 | 2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | unknown |