6FII
Tubulin-Spongistatin complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-04-21 |
Detector | DECTRIS PILATUS 2M-F |
Wavelength(s) | 1.00004 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 105.670, 159.920, 181.010 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.168 - 2.405 |
R-factor | 0.1703 |
Rwork | 0.168 |
R-free | 0.21600 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 4i4t |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX ((dev_2875: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.200 | 2.470 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.167 | 2.734 |
Rmeas | 0.172 | 2.826 |
Number of reflections | 115484 | 8272 |
<I/σ(I)> | 15.8 | 1.06 |
Completeness [%] | 99.8 | 97.5 |
Redundancy | 16.7 | 15.6 |
CC(1/2) | 0.999 | 0.360 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6.7 | 294 | 10 % PEG 4k, 16 % glycerol, 30 mM MgCl2, 30 mM CaCl2, and 100 mM 2-(N-morpholino)ethanesulfonic acid/imidazole |