6EOQ
DPP9 - Apo
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-09-21 |
| Detector | DECTRIS PILATUS 6M-F |
| Wavelength(s) | 0.99997 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 120.370, 118.020, 164.460 |
| Unit cell angles | 90.00, 105.49, 90.00 |
Refinement procedure
| Resolution | 49.260 - 3.000 |
| R-factor | 0.27605 |
| Rwork | 0.273 |
| R-free | 0.33414 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1orv |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.365 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0155) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 49.260 |
| High resolution limit [Å] | 3.000 |
| Number of reflections | 88848 |
| <I/σ(I)> | 5.3 |
| Completeness [%] | 99.8 |
| Redundancy | 13.57 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | 10%PEG 8000, 25% Glycerol, 0.16M Calcium Acetate, 0.08M Caodilate pH6.25, |
