Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
| Synchrotron site | Australian Synchrotron |
| Beamline | MX2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2014-10-09 |
| Detector | ADSC QUANTUM 270 |
| Wavelength(s) | 0.9537 |
| Spacegroup name | P 4 21 2 |
| Unit cell lengths | 109.386, 109.386, 96.963 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 48.919 - 2.198 |
| R-factor | 0.2047 |
| Rwork | 0.203 |
| R-free | 0.23110 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2p1l |
| RMSD bond length | 0.007 |
| RMSD bond angle | 0.806 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.920 | 2.277 |
| High resolution limit [Å] | 2.198 | 2.198 |
| Number of reflections | 30476 | 2914 |
| <I/σ(I)> | 20.63 | |
| Completeness [%] | 99.6 | |
| Redundancy | 14.1 | |
| CC(1/2) | 0.999 | 0.483 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7 | 293 | 0.1M Tris pH 7.0, 0.2M MgCl2, 2.5M NaCl |
