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6C7A

Conformational Changes in a Class A Beta lactamase that Prime it for Catalysis

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 19-ID
Synchrotron siteAPS
Beamline19-ID
Detector technologyCCD
Collection date2015-01-09
DetectorADSC QUANTUM 315r
Wavelength(s)0.97
Spacegroup nameP 32 2 1
Unit cell lengths71.825, 71.825, 96.534
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution48.270 - 1.050
Rwork0.120
R-free0.15000
Data reduction softwareXDS
Data scaling softwareSCALA
Refinement softwareSHELXL
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]48.2701.110
High resolution limit [Å]1.0501.050
Rmerge0.0750.370
Rpim0.0200.149
Number of reflections134116
<I/σ(I)>5.82
Completeness [%]99.999.1
Redundancy9.27.2
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1BATCH MODE6.129310 mg/ml protein in a solution containing 2.0 M ammonium sulfate and 0.1 M sodium citrate (pH 6.1)

219869

PDB entries from 2024-05-15

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