6BW3
Crystal structure of RBBP4 in complex with PRDM3 N-terminal peptide
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-05-10 |
Detector | RIGAKU SATURN A200 |
Wavelength(s) | 1.54178 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 75.979, 59.822, 101.773 |
Unit cell angles | 90.00, 94.55, 90.00 |
Refinement procedure
Resolution | 46.950 - 2.200 |
R-factor | 0.21671 |
Rwork | 0.215 |
R-free | 0.24594 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2xu7 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.476 |
Data reduction software | XDS |
Data scaling software | Aimless (0.5.32) |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0189) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 46.950 | 46.950 | 2.270 |
High resolution limit [Å] | 2.200 | 9.070 | 2.200 |
Rmerge | 0.099 | 0.021 | 0.991 |
Rmeas | 0.114 | 0.025 | 1.141 |
Rpim | 0.056 | 0.014 | 0.559 |
Number of reflections | 46303 | 702 | 3952 |
<I/σ(I)> | 14.3 | ||
Completeness [%] | 99.4 | 97.9 | 98.4 |
Redundancy | 4.1 | 3.7 | 4 |
CC(1/2) | 0.990 | 0.931 | 0.681 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 277 | 20% PEG3350, 0.2 M sodium malonate, 0.1 M BisTris |