6B6F
Beta-Lactamase, mixed with Ceftriaxone, needles crystal form, 2sec
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | FREE ELECTRON LASER |
| Source details | SLAC LCLS BEAMLINE CXI |
| Synchrotron site | SLAC LCLS |
| Beamline | CXI |
| Temperature [K] | 300 |
| Detector technology | PIXEL |
| Collection date | 2016-09-10 |
| Detector | CS-PAD CXI-1 |
| Wavelength(s) | 1.3 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 39.730, 41.690, 69.530 |
| Unit cell angles | 90.00, 104.68, 90.00 |
Refinement procedure
| Resolution | 19.854 - 2.050 |
| R-factor | 0.2023 |
| Rwork | 0.200 |
| R-free | 0.25030 |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.573 |
| Data reduction software | CrystFEL |
| Data scaling software | CrystFEL |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.12_2829: ???)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 19.854 |
| High resolution limit [Å] | 2.050 |
| Number of reflections | 13311 |
| <I/σ(I)> | 5.1 |
| Completeness [%] | 100.0 |
| Redundancy | 238 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | free interface diffustion | 293 | 0.1 M sodium acetate pH 5.0, 45% PEG 1000 |
