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6AB2

Crystal structure of Methanosarcina mazei PylRS(Y306A/Y384F) complexed with oClZLys

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSPRING-8 BEAMLINE BL26B2
Synchrotron siteSPring-8
BeamlineBL26B2
Temperature [K]100
Detector technologyCCD
Collection date2014-10-06
DetectorMARMOSAIC 225 mm CCD
Wavelength(s)1
Spacegroup nameC 1 2 1
Unit cell lengths101.419, 43.887, 72.386
Unit cell angles90.00, 119.45, 90.00
Refinement procedure
Resolution35.071 - 1.400
R-factor0.1712
Rwork0.170
R-free0.19780
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2zim
RMSD bond length0.006
RMSD bond angle1.047
Data reduction softwareXDS
Data scaling softwareXSCALE
Phasing softwarePHASER
Refinement softwarePHENIX ((1.13_2998: ???))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0001.440
High resolution limit [Å]1.4001.400
Rmeas0.058
Rpim0.0210.161
Number of reflections533992623
<I/σ(I)>34.5
Completeness [%]97.5
Redundancy7.6
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP8.5281Tris-HCl (pH 8.5), PEG 200, KCl, MgCl2, sodium citrate

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