5ZSI
Crystal structure of monkey TLR7 in complex with CL097
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE AR-NE3A |
Synchrotron site | Photon Factory |
Beamline | AR-NE3A |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-05-27 |
Detector | DECTRIS PILATUS 2M-F |
Wavelength(s) | 1.0000 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 99.366, 139.951, 149.468 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.683 - 2.700 |
R-factor | 0.2015 |
Rwork | 0.199 |
R-free | 0.25860 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.442 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.770 |
High resolution limit [Å] | 2.700 | 2.700 |
Number of reflections | 57899 | |
<I/σ(I)> | 17 | |
Completeness [%] | 100.0 | |
Redundancy | 13.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | PEG 4000, ammonium sulfate, sodium citrate pH 5.0, Tris-HCl pH 7.5 and NaCl |