5ZND
8-mer nanotube derived from 24-mer rHuHF nanocage
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-01-02 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9779 |
Spacegroup name | I 4 2 2 |
Unit cell lengths | 100.352, 100.352, 51.712 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 33.894 - 3.000 |
R-factor | 0.2323 |
Rwork | 0.227 |
R-free | 0.27560 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2fha |
RMSD bond length | 0.003 |
RMSD bond angle | 0.671 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.050 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.117 | |
Rmeas | 0.124 | |
Number of reflections | 2556 | 134 |
<I/σ(I)> | 19.58 | 6.15 |
Completeness [%] | 90.1 | 100 |
Redundancy | 11.5 | 12.9 |
CC(1/2) | 0.982 | 0.960 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 293 | 0.2M ammonium citrate (pH=8.0), 0.1M Tris-HCl (pH=8.0), 22% (w/v) PEG 3350 |