5ZMN
Sulfur binding domain and SRA domain of ScoMcrA complexed with phosphorothioated DNA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-09-09 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97916 |
Spacegroup name | I 41 2 2 |
Unit cell lengths | 122.340, 122.340, 313.691 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 113.980 - 3.290 |
R-factor | 0.2526 |
Rwork | 0.251 |
R-free | 0.28780 |
RMSD bond length | 0.018 |
RMSD bond angle | 1.792 |
Data scaling software | HKL-2000 |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 113.980 | 3.420 |
High resolution limit [Å] | 3.290 | 3.300 |
Number of reflections | 34877 | |
<I/σ(I)> | 14.1 | |
Completeness [%] | 99.9 | |
Redundancy | 3.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 287 | 2.0M ammonium sulfate, 0.1M CAPS buffer, pH 10.5, 0.2M lithium sulfate |