5YEV
Murine DR3 death domain
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL17U1 |
| Synchrotron site | SSRF |
| Beamline | BL17U1 |
| Temperature [K] | 110 |
| Detector technology | CCD |
| Collection date | 2015-09-20 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.979297 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 91.390, 143.700, 177.350 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 47.640 - 2.500 |
| Rwork | 0.212 |
| R-free | 0.25260 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1omp |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | PHENIX (v1.12-2829) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 47.640 |
| High resolution limit [Å] | 2.500 |
| Number of reflections | 81215 |
| <I/σ(I)> | 7.37 |
| Completeness [%] | 99.8 |
| Redundancy | 7.6606 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 291 | 2 M ammonium sulfate, Sodium citrate 5.6, 5% glycerol |
