5Y6J
Structure of Tomato spotted wilt virus nucleocapsid protein with alternative oligomerization state
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-06-08 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9798 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 55.364, 76.514, 98.440 |
Unit cell angles | 90.00, 93.55, 90.00 |
Refinement procedure
Resolution | 49.492 - 2.811 |
R-factor | 0.2338 |
Rwork | 0.232 |
R-free | 0.27520 |
Structure solution method | SAD |
RMSD bond length | 0.003 |
RMSD bond angle | 0.732 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | HKL-2000 |
Refinement software | PHENIX (1.11.1_2575) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.850 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.471 | |
Number of reflections | 20050 | |
<I/σ(I)> | 21.1 | 4.2 |
Completeness [%] | 99.9 | 99.8 |
Redundancy | 6.2 | 6.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 298 | 0.05 M BIS-TRIS pH 7.0; 22% (v/v) Pentaerythritol ethoxylate (15/4 EO/OH); 20% (v/v) glycerol |