5Y27
Crystal structure of Se-Met Dpb4-Dpb3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-04-01 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.97915 |
Spacegroup name | P 65 |
Unit cell lengths | 86.291, 86.291, 59.710 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 37.365 - 1.900 |
R-factor | 0.1943 |
Rwork | 0.192 |
R-free | 0.24380 |
Structure solution method | SAD |
RMSD bond length | 0.008 |
RMSD bond angle | 1.008 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.970 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.713 | |
Number of reflections | 20156 | 2032 |
<I/σ(I)> | 72 | |
Completeness [%] | 100.0 | 100 |
Redundancy | 49.9 | 50 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 9.5 | 283.15 | PEG 3350, ches |