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5Y04

Crystal Structure of the complex between the vinculin D1 domain and alphaE-catenin

Experimental procedure
Experimental methodMAD
Source typeSYNCHROTRON
Source detailsSPRING-8 BEAMLINE BL41XU
Synchrotron siteSPring-8
BeamlineBL41XU
Temperature [K]100
Detector technologyCCD
Collection date2009-10-19
DetectorRAYONIX MX225HE
Wavelength(s)0.9785, 0.9788, 0.9946
Spacegroup nameP 21 21 2
Unit cell lengths54.807, 73.825, 111.485
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution50.000 - 2.850
R-factor0.248
Rwork0.247
R-free0.28100
Structure solution methodMAD
RMSD bond length0.008
RMSD bond angle1.270
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareSHARP
Refinement softwareREFMAC (5.6.0117)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.950
High resolution limit [Å]2.8502.850
Number of reflections10287
<I/σ(I)>41.42.8
Completeness [%]96.073.4
Redundancy6.74.2
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION8293100MM IMIDAZOLE, 0.5-0.7M POTASSIUM TARTRATE, 0.35M SODIUM FORMATE

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