5XZW
Crystal structure of Rad53 1-466
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSRRC BEAMLINE BL15A1 |
Synchrotron site | NSRRC |
Beamline | BL15A1 |
Temperature [K] | 110 |
Detector technology | CCD |
Collection date | 2014-03-27 |
Detector | RAYONIX MX300HE |
Wavelength(s) | 0.90000 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 115.809, 115.809, 141.269 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 29.528 - 2.800 |
R-factor | 0.2686 |
Rwork | 0.267 |
R-free | 0.28430 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.396 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.900 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.057 | 0.699 |
Number of reflections | 27160 | |
<I/σ(I)> | 19.8 | |
Completeness [%] | 98.6 | 100 |
Redundancy | 9 | 9.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6.5 | 293 | 100MM CACODYLATE, 0.4M NACL, 1.5M (NH4)2SO4 |
1 | VAPOR DIFFUSION | 6.5 | 293 | 100MM CACODYLATE, 0.4M NACL, 1.5M (NH4)2SO4 |