5XY9
Structure of the MST4 and 14-3-3 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-10-11 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9792 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 72.994, 84.734, 111.859 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 34.821 - 2.303 |
R-factor | 0.1985 |
Rwork | 0.195 |
R-free | 0.24510 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1qja |
RMSD bond length | 0.007 |
RMSD bond angle | 0.916 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.340 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.097 | 0.878 |
Number of reflections | 31310 | 1527 |
<I/σ(I)> | 38 | 3 |
Completeness [%] | 99.9 | 99.9 |
Redundancy | 14 | 12.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 289 | 0.2M MgCl2, 0.1M Tris pH 8.5, 25% PEG 3350 |