5XWT

Crystal structure of PTPdelta Ig1-Fn1 in complex with SALM5 LRR-Ig

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SPRING-8 BEAMLINE BL44XU
Synchrotron site	SPring-8
Beamline	BL44XU
Temperature [K]	100
Detector technology	PIXEL
Collection date	2016-05-16
Detector	DECTRIS PILATUS3 S 6M
Wavelength(s)	1
Spacegroup name	P 21 21 21
Unit cell lengths	98.260, 169.753, 210.946
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	49.862 - 4.178
R-factor	0.2633
Rwork	0.261
R-free	0.31130
RMSD bond length	0.002
RMSD bond angle	0.600
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	PHENIX (1.9_1692)

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	3.940
Number of reflections	31657
<I/σ(I)>	13.4
Completeness [%]	99.2
Redundancy	10.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	7% PEG 4000, 0.1M NaCl, 0.1M Li2SO4, 0.1M ADA (pH 6.5)