5XV6
Crystal structure of ATG101-ATG13HORMA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-17A |
Synchrotron site | Photon Factory |
Beamline | BL-17A |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-12-20 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9800 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 84.019, 123.485, 99.798 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.899 - 2.455 |
R-factor | 0.2291 |
Rwork | 0.225 |
R-free | 0.27110 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5xuy |
RMSD bond length | 0.009 |
RMSD bond angle | 1.100 |
Data scaling software | HKL-2000 |
Refinement software | PHENIX (1.10.1_2155) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.480 |
High resolution limit [Å] | 2.440 | 6.620 | 2.440 |
Rmerge | 0.090 | 0.060 | 0.912 |
Rmeas | 0.098 | 0.066 | 0.984 |
Rpim | 0.038 | 0.027 | 0.363 |
Total number of observations | 136207 | ||
Number of reflections | 19228 | ||
<I/σ(I)> | 8.1 | ||
Completeness [%] | 99.6 | 98.4 | 99.3 |
Redundancy | 7.1 | 6.2 | 7.1 |
CC(1/2) | 0.995 | 0.811 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.1M HEPES (pH7.5), 0.2M MgCl2, 6-8% (w/v) PEG 3350 |