5XUP
Crystal structure of TRF1 and TERB1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-05-31 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97853 |
Spacegroup name | P 64 |
Unit cell lengths | 161.579, 161.579, 45.925 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 46.690 - 2.100 |
R-factor | 0.179 |
Rwork | 0.177 |
R-free | 0.22070 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3bqo |
RMSD bond length | 0.006 |
RMSD bond angle | 0.985 |
Data scaling software | HKL-2000 |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.180 |
High resolution limit [Å] | 2.100 | 4.520 | 2.100 |
Rmerge | 0.121 | 0.073 | 0.755 |
Rmeas | 0.127 | 0.077 | 0.797 |
Rpim | 0.040 | 0.025 | 0.254 |
Total number of observations | 402507 | ||
Number of reflections | 40395 | ||
<I/σ(I)> | 3.1 | ||
Completeness [%] | 100.0 | 100 | 100 |
Redundancy | 10 | 9.6 | 9.8 |
CC(1/2) | 0.995 | 0.831 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 8.5 | 289 | 10% 2-propanol, 0.1M Tris-HCl |