5XSD
XylFII-LytSN complex mutant - D103A
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-09-23 |
Detector | RAYONIX MX-225 |
Wavelength(s) | 0.9798 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 144.958, 144.958, 103.074 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.644 - 2.500 |
R-factor | 0.2305 |
Rwork | 0.229 |
R-free | 0.25330 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.011 |
RMSD bond angle | 2.028 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.500 |
Number of reflections | 38385 |
<I/σ(I)> | 20.46 |
Completeness [%] | 99.7 |
Redundancy | 5.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 293 | 0.1 M Lithium sulfate, 0.1 M Sodium citrate tribasic dihydrate pH 5.5, 20% w/v Polyethylene glycol 1000 |