5XPD
Sugar transporter of AtSWEET13 in inward-facing state with a substrate analog
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-12-09 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9778 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 75.780, 42.831, 116.553 |
Unit cell angles | 90.00, 93.85, 90.00 |
Refinement procedure
Resolution | 36.684 - 2.788 |
R-factor | 0.2513 |
Rwork | 0.247 |
R-free | 0.28210 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5CTG and 1FHH |
RMSD bond length | 0.005 |
RMSD bond angle | 0.962 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (dev_1819) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.788 |
Rmerge | 0.148 |
Number of reflections | 9248 |
<I/σ(I)> | 5.8 |
Completeness [%] | 96.3 |
Redundancy | 2.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | LIPIDIC CUBIC PHASE | 5.9 | 293 | 100mM MES (pH 5.9), 38% (w/v) PEG 600, 100mM KH2PO4 |