5X8M

PD-L1 in complex with durvalumab

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 7A (6B, 6C1)
Synchrotron site	PAL/PLS
Beamline	7A (6B, 6C1)
Temperature [K]	100
Detector technology	CCD
Collection date	2016-12-04
Detector	ADSC QUANTUM 270
Wavelength(s)	1.00
Spacegroup name	P 21 21 21
Unit cell lengths	39.950, 97.395, 153.564
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	46.419 - 2.661
R-factor	0.1829
Rwork	0.181
R-free	0.21900
RMSD bond length	0.008
RMSD bond angle	1.105
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	PHENIX (1.9_1692)

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.660
Number of reflections	17827
<I/σ(I)>	16.5
Completeness [%]	99.4
Redundancy	3.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	0.2M Ammonium sulfate, 0.1M Bis-Tris pH 5.5, 25% w/v PEG 3350