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5WR4

Thermolysin, SFX unliganded form with oil-based carrier

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeFREE ELECTRON LASER
Source detailsSACLA BEAMLINE BL3
Synchrotron siteSACLA
BeamlineBL3
Temperature [K]300
Detector technologyCCD
Collection date2015-05-19
DetectorMPCCD
Wavelength(s)1.77
Spacegroup nameP 61 2 2
Unit cell lengths93.670, 93.670, 130.950
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution46.800 - 2.100
R-factor0.152
Rwork0.150
R-free0.18800
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)4ow3
Data reduction softwareCrystFEL
Data scaling softwareCrystFEL
Phasing softwarePHENIX
Refinement softwarePHENIX
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]46.8002.170
High resolution limit [Å]2.1002.100
Number of reflections20468
<I/σ(I)>4.82.1
Completeness [%]100.0100
Redundancy137.839.6
CC(1/2)0.9230.637
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1BATCH MODE6.5277PEG2000MME, MES, CaCl2

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