5WA1
CHMP4C A232T in complex with ALIX BRO1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL12-2 |
Synchrotron site | SSRL |
Beamline | BL12-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-03-13 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9794 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 120.979, 61.450, 76.187 |
Unit cell angles | 90.00, 121.70, 90.00 |
Refinement procedure
Resolution | 37.811 - 1.868 |
R-factor | 0.1946 |
Rwork | 0.194 |
R-free | 0.21500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3c3r |
RMSD bond length | 0.005 |
RMSD bond angle | 0.717 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.811 | 1.935 |
High resolution limit [Å] | 1.868 | 1.868 |
Rmerge | 0.022 | 0.808 |
Number of reflections | 38802 | 3744 |
<I/σ(I)> | 8.78 | 0.97 |
Completeness [%] | 97.6 | 93.38 |
Redundancy | 2 | |
CC(1/2) | 0.999 | 0.600 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 293.15 | 15% PEG8000, 100 mM MES, pH 6.5, 200 mM sodium acetate |