5W9S
Zinc finger of human CXXC5 in complex with CpG DNA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2012-08-22 |
Detector | RIGAKU |
Wavelength(s) | 1.5418 |
Spacegroup name | P 32 |
Unit cell lengths | 40.110, 40.110, 81.200 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 34.740 - 2.100 |
R-factor | 0.2202 |
Rwork | 0.218 |
R-free | 0.25370 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4hp3 |
RMSD bond length | 0.015 |
RMSD bond angle | 1.744 |
Data reduction software | Aimless (0.5.27) |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0155) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 34.740 | 34.740 | 2.160 |
High resolution limit [Å] | 2.100 | 8.910 | 2.100 |
Rmerge | 0.040 | 0.021 | 1.013 |
Rmeas | 0.042 | 0.022 | 1.061 |
Rpim | 0.012 | 0.007 | 0.315 |
Total number of observations | 96584 | 1196 | 7833 |
Number of reflections | 8535 | ||
<I/σ(I)> | 34.9 | 112 | 2.6 |
Completeness [%] | 100.0 | 99.7 | 100 |
Redundancy | 11.3 | 10.3 | 11.1 |
CC(1/2) | 1.000 | 1.000 | 0.774 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6.5 | 291 | 30% PEG-5000-MME, 0.2M ammonium sulfate, 0.1M MES |