Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALS BEAMLINE 8.2.2 |
| Synchrotron site | ALS |
| Beamline | 8.2.2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2007-10-04 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.98 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 96.620, 101.252, 128.182 |
| Unit cell angles | 90.00, 90.63, 90.00 |
Refinement procedure
| Resolution | 47.430 - 2.800 |
| R-factor | 0.226 |
| Rwork | 0.224 |
| R-free | 0.27000 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2r5h |
| RMSD bond length | 0.016 |
| RMSD bond angle | 1.469 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | MOLREP |
| Refinement software | PHENIX (1.8.4_1496) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 47.426 | 2.900 |
| High resolution limit [Å] | 2.797 | 2.800 |
| Rmerge | 0.082 | 0.353 |
| Number of reflections | 60092 | |
| <I/σ(I)> | 14.28 | |
| Completeness [%] | 98.5 | |
| Redundancy | 2.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 291 | 30% PEG400, 0.1 M MES |
