5VWX
Bak core latch dimer in complex with Bim-h0-h3Glt
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 77 |
Detector technology | PIXEL |
Collection date | 2017-03-02 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9464 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 61.629, 76.481, 77.546 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.248 - 2.489 |
R-factor | 0.2557 |
Rwork | 0.250 |
R-free | 0.30470 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.002 |
RMSD bond angle | 0.416 |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.10.1_2155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.250 | |
High resolution limit [Å] | 2.489 | 2.489 |
Rmerge | 0.165 | |
Number of reflections | 13253 | |
<I/σ(I)> | 8.51 | |
Completeness [%] | 98.0 | |
Redundancy | 7.3 | |
CC(1/2) | 0.997 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5 | 281 | 200 mM calcium acetate, 30 % PEG 400 and 100 mM sodium acetate-acetic acid pH 5.0 |