5VWV
Bak core latch dimer in complex with Bim-BH3 - Cubic
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-07-12 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9537 |
Spacegroup name | P 41 3 2 |
Unit cell lengths | 139.404, 139.404, 139.404 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.032 - 1.897 |
R-factor | 0.1579 |
Rwork | 0.157 |
R-free | 0.17710 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 0.755 |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.10.1_2155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.032 | 1.966 |
High resolution limit [Å] | 1.897 | 1.898 |
Rmerge | 0.216 | |
Number of reflections | 37157 | 3647 |
<I/σ(I)> | 24.26 | 1.48 |
Completeness [%] | 100.0 | 100 |
Redundancy | 47.8 | 47 |
CC(1/2) | 0.497 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 281 | 18 % glycerol, 21.6 % PEG (poly-ethylene glycol) 1500 and 0.5 % ethyl acetate |