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5V68

Crystal structure of cell division protein FtsZ from Mycobacterium tuberculosis bounded via the T9 loop

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsNSLS BEAMLINE X25
Synchrotron siteNSLS
BeamlineX25
Temperature [K]100
Detector technologyPIXEL
Collection date2013-11-01
DetectorDECTRIS PILATUS 6M
Wavelength(s)1.0781
Spacegroup nameP 21 21 21
Unit cell lengths73.110, 180.850, 220.160
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution55.050 - 3.460
R-factor0.24636
Rwork0.243
R-free0.30860
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2q1y
RMSD bond length0.011
RMSD bond angle1.470
Data reduction softwareXDS
Data scaling softwareXSCALE
Phasing softwarePHENIX
Refinement softwareREFMAC (5.8.0151)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]55.0503.550
High resolution limit [Å]3.4603.460
Rmerge0.0890.614
Rpim0.0530.366
Number of reflections372872754
<I/σ(I)>9.31.8
Completeness [%]96.497.3
Redundancy3.33.3
CC(1/2)0.9970.735
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP5.62930.1M sodium citrate pH 5.6, 0.3M ammonium acetate, 15% PEG 4000. Protein concentration 3mg/ml. Incubated with 5mM SB-P17-A20

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