5V58

Crystal structure of human prolyl-tRNA synthetase in complex with Aze-SA

Refinement Statistics

Experimental method:X-RAY DIFFRACTION (2.59 Å)

Cell axes86.76686.766108.773
Cell angles90.0090.00120.00
SpacegroupP 32 2 1
Resolution limits35.54 - 2.59
the highest resolution shell value2.655 - 2.588
R-factor0.2291
R-work0.22680
the highest resolution shell value0.291
R-free0.27200
the highest resolution shell value0.335
RMSD bond length0.004
RMSD bond angle1.045

Data Collection Statistics

Resolution limits50.00 - 2.59
the highest resolution shell value -
Number of reflections14793
Rmerge_l_obs0.057
the highest resolution shell value0.337
Completeness96.9
Redundancy10.2
the highest resolution shell value8.1

Crystallization Conditions

crystal IDmethodpHpH rangetemperatureunit
1EVAPORATION293

Crystallization Reagents

IDcrystal IDsolution IDreagent nameconcentrationdetails
Crystallization Reagents in Literatures*
IDcrystal IDsolutionreagent nameconcentration (unit)details
Annotated Information is extracted from Literature Info*